(S)-4-苯基-2-恶唑烷酮合成路线 (共 54 条)
反应条件
pyrrolidin-3-ol in tetrahydrofuran; N,N-dimethyl-formamide T=45 - 55°C;
参考文献
Chemical communications (Cambridge, England), , # 15 p. 1644 - 1645
反应条件
(R)-2-phenyl-1,2-dihydroimidazo[1,2-a]quinoline; N-ethyl-N,N-diisopropylamine in chloroform T=0°C; 3.5 h; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 128, # 20 p. 6536 - 6537
反应条件
Rh2(S-TCPTAD)4; potassium carbonate in dichloromethane T=23°C; 4 h; Title compound not separated from byproducts;
参考文献
Organic Letters, , vol. 8, # 22 p. 5013 - 5016
反应条件
1: t-BuONa / tetrahydrofuran 2: i-Pr2NEt; Na2SO4; (R)-BTM / CHCl3 / 8.5 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 20 p. 6536 - 6537
反应条件
1: NaBH4; LiCl / tetrahydrofuran 2: t-BuONa / tetrahydrofuran 3: i-Pr2NEt; Na2SO4; (R)-BTM / CHCl3 / 8.5 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 20 p. 6536 - 6537
反应条件
1: 91 percent / tetrahydrofuran 2: 84 percent / Et3N / CH2Cl2 3: tetrahydrofuran; dimethylformamide / Heating View Scheme
参考文献
Chemical communications (Cambridge, England), , # 15 p. 1644 - 1645
反应条件
1: 84 percent / Et3N / CH2Cl2 2: tetrahydrofuran; dimethylformamide / Heating View Scheme
参考文献
Chemical communications (Cambridge, England), , # 15 p. 1644 - 1645
反应条件
lithium hydroxide; dihydrogen peroxide
参考文献
Lin, Jun; Liao, Subo; Hruby, Victor J.
Tetrahedron Letters, 1998 , vol. 39, # 20 p. 3117 - 3120
反应条件
lithium hydroxide; dihydrogen peroxide
参考文献
Lin, Jun; Liao, Subo; Hruby, Victor J.
Tetrahedron Letters, 1998 , vol. 39, # 20 p. 3117 - 3120
反应条件
thionyl chloride; triethylamine in dichloromethane
参考文献
Chemical communications (Cambridge, England), , # 15 p. 1644 - 1645