in neat (no solvent) byproducts: (t-C4H9)(i-C3H7)PSiCl3, (t-C4H9)(i-C3H7)PSi2Cl5; N2 atmosphere, addn. of Si2Cl6 to ice-cooled stannyl compound, warming to room temp., 60 min; variation of reaction time; (119)Sn- and (31)P-NMR-monitoring;
参考文献
European Journal of Inorganic Chemistry, , # 8 p. 1381 - 1392