in neat (no solvent) mixt. heated at 150°C for 15 h in a sealed evacuated ampoule; volatiles removed (vac., 100°C) and collected in a trap, residue treated with heptane, cooled to -5°C (crystn.);
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1: NEt3 / pentane 2: NEt3 / pentane 3: not given View Scheme
参考文献
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Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , p. 2002 - 2008
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Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.8, page 76 - 79
Zavgorodnii, V. S.; Sivenkov, E. S.; Petrov, A. A.
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Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.2.7, page 206 - 218
