反应条件
in diethyl ether
Ar atmosphere; addn. of Zn-compd. to soln. of Fe-compd. in diethyl ether (-10°C), stirring (30 h), cooling (-30°C); addn. of soln. of KF in H2O, sepn. of org. layer, washing (water), drying (MgSO4), filtn., removal of Et2O, removal of Fe(C5H5)2 (5 Torr,150°C), distn. (vac.); elem. anal.;
参考文献
Krueger, CH.; Thiele, K.-H.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1989 , vol. 569, p. 97 - 105
