二(三正丁基甲锡烷基)乙炔合成路线 （共 27 条）
参考文献
Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.1, page 38 - 56
反应条件
in neat (no solvent) dropwise addn. of 2 equiv. stannane to Et2BCl at -40°C, stirring at -40°C for 60 min; distn. into cold trap (0.001 Torr);
参考文献
Wrackmeyer; Schanz; Milius
Angewandte Chemie - International Edition in English, 1997 , vol. 36, # 10 p. 1117 - 1119
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=100°C; Stille coupling; 2 h; Inert atmosphere;
参考文献
Brown, Amy E.; Eichler, Barrett E.
Tetrahedron Letters, 2011 , vol. 52, # 16 p. 1960 - 1963
反应条件
2,6-di-tert-butyl-4-methyl-phenol; tetrakis(triphenylphosphine) palladium(0) in toluene 16 h; Heating;
参考文献
Wang, Zhaohui; Doetz, Florian; Enkelmann, Volker; Muellen, Klaus
Angewandte Chemie - International Edition, 2005 , vol. 44, # 8 p. 1247 - 1250
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=100°C; Stille coupling; 2 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 52, # 16 p. 1960 - 1963
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=100°C; Stille coupling; 2 h; Inert atmosphere;
参考文献
Brown, Amy E.; Eichler, Barrett E.
Tetrahedron Letters, 2011 , vol. 52, # 16 p. 1960 - 1963
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=100°C; Stille coupling; 2 h; Inert atmosphere;
参考文献
Brown, Amy E.; Eichler, Barrett E.
Tetrahedron Letters, 2011 , vol. 52, # 16 p. 1960 - 1963
反应条件
2,6-di-tert-butyl-4-methyl-phenol; lithium chloride; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane 5 h; Heating;
参考文献
Chabre, Yoann M.; Brisebois, Patrick P.; Abbassi, Leila; Kerr, Sheena C.; Fahy, John V.; Marcotte, Isabelle; Roy, Rene
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 724 - 727
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=100°C; Stille coupling; 6 h; Inert atmosphere;
参考文献
Brown, Amy E.; Eichler, Barrett E.
Tetrahedron Letters, 2011 , vol. 52, # 16 p. 1960 - 1963
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=100°C; Stille coupling; 4 h; Inert atmosphere;
参考文献
Brown, Amy E.; Eichler, Barrett E.
Tetrahedron Letters, 2011 , vol. 52, # 16 p. 1960 - 1963
