反应条件
sec.-butyllithium; trifluoroacetic acid 1.) THF, cyclohexane, -78 deg C, 0.5 h, -20 deg C, 1 h; 2.) 0 deg C, 13 h; Yield given. Multistep reaction;
参考文献
Desmond, R.; Mills, S. G.; Volante, R. P.; Shinkai, I.
Tetrahedron Letters, 1988 , vol. 29, # 32 p. 3895 - 3898