N-(7-羟基-4-甲基-2-氧代-2H-苯并吡喃-6-基)十六烷酰胺合成路线 （共 6 条）
反应条件
pyridine
T=20°C; 3 h;
参考文献
Wiederschain, German Ya.; Kozlova, Inna K.; Ilyina, Galina S.; Mikhaylova, Margarita A.; Beyer, Elena M.
Carbohydrate Research, 1992 , vol. 224, p. 255 - 272
反应条件
potassium hydroxide in ethanol
pH 10-11;
参考文献
Kozlova, I. K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 7 p. 750 - 753
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , # 7 p. 906 - 909
反应条件
1: 98 percent / pyridine / 3 h / 20 °C
2: 95 percent / 5percent KOH / ethanol / pH 10-11
View Scheme
参考文献
Kozlova, I. K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 7 p. 750 - 753
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , # 7 p. 906 - 909
反应条件
1: 65 percent / nitronium tetrafluoroborate / acetonitrile / 0.5 h / 0 °C
2: 98 percent / Na2S2O4 / aq. NH3 / 0.25 h / Heating
3: 98 percent / pyridine / 3 h / 20 °C
4: 95 percent / 5percent KOH / ethanol / pH 10-11
View Scheme
参考文献
Kozlova, I. K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 7 p. 750 - 753
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , # 7 p. 906 - 909
反应条件
1: 98 percent / Na2S2O4 / aq. NH3 / 0.25 h / Heating
2: 98 percent / pyridine / 3 h / 20 °C
3: 95 percent / 5percent KOH / ethanol / pH 10-11
View Scheme
参考文献
Kozlova, I. K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 7 p. 750 - 753
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , # 7 p. 906 - 909
反应条件
1: 1) sodium ethoxide / 1) ethanol, 2) DMSO, oxolane, 20h, reflux
2: sodium methoxide
View Scheme
参考文献
Wiederschain, German Ya.; Kozlova, Inna K.; Ilyina, Galina S.; Mikhaylova, Margarita A.; Beyer, Elena M.
Carbohydrate Research, 1992 , vol. 224, p. 255 - 272
