(E)-3-乙氧基丙烯酰氯合成路线 （共 10 条）
反应条件
With thionyl chloride T=50°C; 2 h;
参考文献
Weiguny, Jens; Schaefer, Hans J. Liebigs Annalen der Chemie, 1994 , # 3 p. 225 - 234
参考文献
Soc.Usines Chim.Rhone-Poulenc Patent: US2768174 , 1956 ;
反应条件
in 1,2-dichloro-ethane 14 h; Heating;
参考文献
Ziegler, Thomas; Moehler, Hans; Effenberger, Franz Chemische Berichte, 1987 , vol. 120, p. 373 - 378
反应条件
Multi-step reaction with 2 steps 1: benzene / 0.5 h / 10 °C2: 85 percent / benzene / 0.5 h / 10 °C
参考文献
Marquez, Victor E.; Lim, Mu-Ill; Treanor, Susan P.; Plowman, Jacqueline; Priest, Matthew A.; et al. Journal of Medicinal Chemistry, 1988 , vol. 31, # 9 p. 1687 - 1694
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209273', constants.ctx, '0')">thionyl chloride</a> <br />T=50°C; 2 h; <br />
参考文献
Weiguny, Jens; Schaefer, Hans J. Liebigs Annalen der Chemie, 1994 , # 3 p. 225 - 234
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209273', constants.ctx, '0')">thionyl chloride</a> <br />T=80°C; 1.25 h; <br /> <br />
参考文献
SCHERING CORPORATION Patent: WO2009/140342 A1, 2009 ; Location in patent: Page/Page column 118-119 ;
反应条件
T=0 - 20°C; 14 h; <br />
参考文献
Fernandez; Garcia-Mera; Morales; Rodriguez-Borges Synthesis, 2001 , # 2 p. 239 - 242
反应条件
<b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br /> <br /> <br />
参考文献
BASF Aktiengesellschaft Patent: US6392058 B1, 2002 ;
反应条件
<b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br /> <br /> <br />
参考文献
BASF Aktiengesellschaft Patent: US5543568 A1, 1996 ;
反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1: 53 percent / NaOH / H<sub>2</sub>O / 1 h / Heating<br />2: 0.35 g / SOCl<sub>2</sub> / diethyl ether / 4 h / Heating<br /> <br />
参考文献
Moon, Hyung Ryong; Kim, Hea Ok; Chun, Moon Woo; Jeong, Lak Shin; Marquez, Victor E. Journal of Organic Chemistry, 1999 , vol. 64, # 13 p. 4733 - 4741
