2,6-二氯-4-三氟甲基磺酰基苯胺合成路线 （共 3 条）
反应条件
[bmim]BF4; trichloroisocyanuric acid; water
T=20°C; 0.0833333 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Journal of Fluorine Chemistry, 2007 , vol. 128, # 6 p. 636 - 640
反应条件
1: 98 percent / iron; hydrochloric acid / H2O / 1 h / 90 °C
2: 96 percent / trichloroisocyanuric acid; [Bmim]BF4; H2O / 0.08 h / 20 °C
View Scheme
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Journal of Fluorine Chemistry, 2007 , vol. 128, # 6 p. 636 - 640
反应条件
1: 68 percent / Na2HPO4; HOCH2SO2Na / dimethylformamide; H2O / 2.5 h / 20 °C / 9000.9 Torr
2: 98 percent / iron; hydrochloric acid / H2O / 1 h / 90 °C
3: 96 percent / trichloroisocyanuric acid; [Bmim]BF4; H2O / 0.08 h / 20 °C
View Scheme
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Journal of Fluorine Chemistry, 2007 , vol. 128, # 6 p. 636 - 640
