3-氨基-4-硝基苯甲酸甲酯合成路线 （共 3 条）
反应条件
1.1: SOCl2 / dimethylformamide / 3 h / Heating 2.1: NaN3 / acetone; H2O / 0.25 h / 20 °C 3.1: 2-(trimethylsilyl)ethanol / xylene / 16 h / Heating 3.2: TBAF / tetrahydrofuran / 0.5 h / 20 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 19 p. 2759 - 2770
反应条件
FeCl3·6H2O; carbon; hydrazine hydrate in methanol 2 h; Reflux;
参考文献
Wetzel, Alexander; Gagosz, Fabien
Angewandte Chemie - International Edition, 2011 , vol. 50, # 32 p. 7354 - 7358
反应条件
1: tetrahydrofuran / 1 h / 20 °C 2: BH3*DMS / tetrahydrofuran / 3 h / 2 °C View Scheme
参考文献
Hay, Michael P.; Sykes, Bridget M.; Denny, William A.; O'Connor, Charmian J.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 19 p. 2759 - 2770
