4-氨基-5-异丙基-5-甲基-2(5H)-呋喃酮合成路线 (共 3 条)
反应条件
lithium hexamethyldisilazane in tetrahydrofuran
T=-78°C; 2 h;
参考文献
Hiyama; Oishi; Suetsugu; et al.
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 6 p. 2139 - 2150
反应条件
1: 1.) ZnI2, 2.) FeCl3
2: 62 percent / LiN(SiMe3)2 / tetrahydrofuran / 2 h / -78 °C
View Scheme
参考文献
Hiyama, Tamejiro; Oishi, Haruhito; Saimoto, Hiroyuki
Tetrahedron Letters, 1985 , vol. 26, # 20 p. 2459 - 2462
反应条件
1: iron(III) chloride / 1 h / 0 deg C to room temp.
2: 62 percent / LiN(SiMe3)2 / tetrahydrofuran / -78 °C
View Scheme
参考文献
Hiyama; Oishi; Suetsugu; et al.
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 6 p. 2139 - 2150