2-(3-溴苯基)-1,3-苯并恶唑合成路线 （共 10 条）
反应条件
Na8H[PW9O34]*7H2O in acetonitrile
T=25°C; 6 h;
参考文献
Zhao, Shen; Chen, Yang; Song, Yu-Fei
Applied Catalysis A: General, 2014 , vol. 475, p. 140 - 146
反应条件
caesium carbonate; copper(l) iodide; 1,10-phenanthroline in 1,4-dioxane
T=120°C; 24 h; Inert atmosphere; Product distribution / selectivity;
参考文献
NITTO DENKO CORPORATION
Patent: US2012/226046 A1, 2012 ;
Location in patent: Page/Page column 22 ;
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate) in toluene
T=80°C; 3 h;
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
potassium carbonate; copper(II) oxide in dimethyl sulfoxide
T=110°C; 24 h;
参考文献
Saha, Prasenjit; Ramana, Tamminana; Purkait, Nibadita; Ali, Md. Ashif; Paul, Rajesh; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8719 - 8725
反应条件
(R)-(+)-1,1'-binaphthyl-2,2'-diamine; copper(II) bis(trifluoromethanesulfonate); caesium carbonate in acetonitrile
T=82°C; Ullmann type intramolecular coupling; 36 h; Inert atmosphere;
参考文献
Naidu, Ajay B.; Sekar, Govindasamy
Synthesis, 2010 , # 4 art. no. Z20609SS, p. 579 - 586
反应条件
toluene-4-sulfonic acid in xylene
6 h; Heating;
参考文献
Johnson, Steven M.; Connelly, Stephen; Wilson, Ian A.; Kelly, Jeffery W.
Journal of Medicinal Chemistry, 2008 , vol. 51, # 2 p. 260 - 270
反应条件
di-tert-butyl peroxide; FeBr2
T=110°C; Inert atmosphere;
参考文献
Gu, Lijun; Jin, Cheng; Guo, Junming; Zhang, Lizhu; Wang, Wei
Chemical Communications, 2013 , vol. 49, # 93 p. 10968 - 10970
反应条件
1: hydrazine / methanol; chloroform; water / 12 h / 20 °C
2: acetic acid / water / 0.5 h / 20 °C
3: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3 h / 80 °C
View Scheme
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
1: acetic acid / water / 0.5 h / 20 °C
2: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3 h / 80 °C
View Scheme
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
1: pyridine; copper(I) bromide / dichloromethane / 48 h / 20 °C / Molecular sieve
2: hydrazine / methanol; chloroform; water / 12 h / 20 °C
3: acetic acid / water / 0.5 h / 20 °C
4: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3 h / 80 °C
View Scheme
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
