man verseift den entstehenden Ester mit waessr.Kalilauge und wenig Alkohol; inactive propane-α.α.β-tricarboxylic acid;
参考文献
Bischoff; Guthzeit
Chemische Berichte, 1881 , vol. 14, p. 616
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Bischoff
Chemische Berichte, 1880 , vol. 13, p. 2163
Justus Liebigs Annalen der Chemie, 1882 , vol. 214, p. 61
Gresham et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 2345
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Goodrich Co.
Patent: US2705243 , 1950 ;
ethanol
Erwaermen des Reaktionsprodukts mit wss.-aethanol.Kalilauge und Erhitzen des nach dem Ansaeuern erhaltenen Reaktionsprodukts unter vermindertem Druck bis auf 170grad;
Cl2Ni(1,2-bis(diphenylphosphino)ethane); isopropylmagnesium chloride in tetrahydrofuran
24 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. C21 - C24
Cl2Ni(1,2-bis(diphenylphosphino)ethane); isopropylmagnesium chloride in tetrahydrofuran
36 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. C21 - C24
Cl2Ni(1,2-bis(diphenylphosphino)ethane); isopropylmagnesium chloride in tetrahydrofuran
24 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. C21 - C24
