4-(吡唑-1-基)苯甲醛合成路线 （共 9 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=120°C; 5 h;
参考文献
Tanaka, Akira; Terasawa, Takeshi; Hagihara, Hiroyuki; Sakuma, Yuri; Ishibe, Noriko; Sawada, Masae; Takasugi, Hisashi; Tanaka, Hirokazu
Journal of Medicinal Chemistry, 1998 , vol. 41, # 13 p. 2390 - 2410
反应条件
potassium carbonate; bis(μ-iodo)bis[(-)-sparteine]dicopper(I) in dimethyl sulfoxide T=115°C; 8 h;
参考文献
Maheswaran; Krishna, G. Gopi; Prasanth, K. Leon; Srinivas; Chaitanya, G. Krishna; Bhanuprakash
Tetrahedron, 2008 , vol. 64, # 10 p. 2471 - 2479
反应条件
potassium carbonate; bis(μ-iodo)bis[(-)-sparteine]dicopper(I) in dimethyl sulfoxide T=125°C; 18 h;
参考文献
Maheswaran; Krishna, G. Gopi; Prasanth, K. Leon; Srinivas; Chaitanya, G. Krishna; Bhanuprakash
Tetrahedron, 2008 , vol. 64, # 10 p. 2471 - 2479
反应条件
pyridinium chlorochromate in dichloromethane 1.5 h; Ambient temperature;
参考文献
Artico; Silvestri; Stefancich; Avigliano; Di Giulio; Maccarrone; Agostinelli; Mondovi; Morpurgo
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 3 p. 219 - 228
反应条件
Cu-exchanged fluoroapatite; air in methanol T=20°C; 13 h;
参考文献
Kantam, Mannepalli Lakshmi; Venkanna, Gopaladasu Tirupati; Kumar, Kota Balaji Shiva; Subrahmanyam, Vura Bala
Helvetica Chimica Acta, 2010 , vol. 93, # 5 p. 974 - 979
反应条件
1: 89 percent / NaBH4, CaCl2 / tetrahydrofuran / Ambient temperature 2: 88 percent / pyridinium chlorochromate (PCC) / CH2Cl2 / 1.5 h / Ambient temperature View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 27, # 3 p. 219 - 228
反应条件
1: 74 percent / NaH / dimethylsulfoxide / 18 h / 100 °C 2: 89 percent / NaBH4, CaCl2 / tetrahydrofuran / Ambient temperature 3: 88 percent / pyridinium chlorochromate (PCC) / CH2Cl2 / 1.5 h / Ambient temperature View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 27, # 3 p. 219 - 228
反应条件
1: 84 percent / K2CO3 / dimethylsulfoxide / 16 h / 120 °C 2: 55 percent / DIBAL-H / toluene / -60 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 11 p. 2955 - 2959
反应条件
palladium diacetate; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in acetone T=50°C; Inert atmosphereGlovebox;
参考文献
Tschaen, Brittany A.; Schmink, Jason R.; Molander, Gary A.
Organic Letters, 2013 , vol. 15, # 3 p. 500 - 503
