2-(2-氨基乙基氨基)-吡啶二盐酸盐合成路线 (共 3 条)
反应条件
hydrogenchloride in 1,4-dioxane; dichloromethane
T=0 - 20°C;
参考文献
Keenan, Richard M.; Miller, William H.; Barton, Linda S.; Bondinell, William E.; Cousins, Russell D.; Eppley, Daniel F.; Hwang, Shing-Mei; Kwon, Chet; Lago, M. Amparo; Nguyen, Thomas T.; Smith, Brian R.; Uzinskas, Irene N.; Yuan, Catherine C. K.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 13 p. 1801 - 1806
反应条件
1: 78 percent / cyclohexene / 10 percent Pd/C / propan-2-ol / Heating
2: 95 percent / 4 N HCl / dioxane; CH2Cl2 / 0 - 20 °C
View Scheme
参考文献
Keenan, Richard M.; Miller, William H.; Barton, Linda S.; Bondinell, William E.; Cousins, Russell D.; Eppley, Daniel F.; Hwang, Shing-Mei; Kwon, Chet; Lago, M. Amparo; Nguyen, Thomas T.; Smith, Brian R.; Uzinskas, Irene N.; Yuan, Catherine C. K.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 13 p. 1801 - 1806
反应条件
hydrogenchloride
8 h; Heating;
参考文献
Mega, Tomohiro; Hamazume, Yasuki; Ikenaka, Tokuji
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 4315 - 4322