反应条件
in neat (no solvent) Electric Arc; mixt. vac. baking at 1800°C for 3 h, arc burning (20 A) for 20 min; soot extn. with toluene for 5 h, pyridine addn., N2 flowing into mixt. in stainless steel tube for ca. 1 h, tube sealing (N2), baking at 200°C for 5 h, sludge filtration, washing; anal. by LDI/TOF/MS;
参考文献
Journal of Physical Chemistry B, , vol. 101, # 20 p. 3927 - 3930
