Vyazankin, N. S.; Razuvaev, G. A.; Korneva, S. P.
J. Gen. Chem. USSR, 1964 , vol. 34, p. 2809 - 2812
Zh. Obsahch. Khim., 1964 , vol. 34, p. 2787 - 2791
in diethyl ether; cyclohexane
byproducts: i-Pr2NH; Et3SnH in Et2O cooled to 0°C under Ar, LDA in cyclohexane (1.6 M) added via syringe, stirred for 60 min at room temp., hydrolysis;
参考文献
Reimann, Werner; Kuivila, Henry G.; Farah, Dan; Apoussidis, Theodorus
Organometallics, 1987 , vol. 6, p. 557 - 565
azodiisobutyric acid dinitrile in not given
byproducts: C6H5OH;
参考文献
Creemers, H. M. J. C.; Verbeek, F.; Noltes, J. G.
Journal of Organometallic Chemistry, 1967 , vol. 8, p. 469 - 477
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.5, page 34 - 36
azodiisobutyric acid dinitrile in further solvent(s)
byproducts: C6H6, (C2H5)(CH3)NH, CH4; reaction for 6 h at 80°C in cumol in presence of azoisobutyric acid dinitrile;;
参考文献
Hollaender, J.; Neumann, W. P.
Angewandte Chemie, 1971 , vol. 83, p. 850 - 851
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.2, page 22 - 31
→
反应条件
azodiisobutyric acid dinitrile in further solvent(s)
byproducts: C6H6, (NH2)(C2H5)NH, NH3; reaction for 6 h at 80°C in cumol in presence of azoisobutyric acid dinitrile;;
参考文献
Hollaender, J.; Neumann, W. P.
Angewandte Chemie, 1971 , vol. 83, p. 850 - 851
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.2, page 22 - 31
