1,2-二亚油酰基-sn-甘油-3-磷酸胆碱合成路线 (共 6 条)
反应条件
air; potassium chloride; water; tetraethylammonium hydroxide; triphenylphosphine multistep reaction: 1) 37 deg C, 22 h, CHCl3; 2) aq. ether; title compound was oxidized also in mixtures with varying proportions of 1,2-dipalmitoylglycerophosphatidylcholine; Product distributionMechanism;
参考文献
Porter, Ned A.; Weber, Bruce A.; Weenen, Hugo; Khan, Jamil A.
Journal of the American Chemical Society, 1980 , vol. 102, # 17 p. 5597 - 5601
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane
T=20°C; 40 h; Inert atmosphere;
参考文献
Niezgoda, Natalia; Mitula, Pawel; Kempinska, Katarzyna; Wietrzyk, Joanna; Wawrzenczyk, Czeslaw
Australian Journal of Chemistry, 2013 , vol. 66, # 3 p. 354 - 361
反应条件
pyridine in chloroform
参考文献
Shvets,V.I. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, p. 1908 - 1911,1921 - 1923
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Baba, Naomichi; Akiyama, Takeshi; Tahara, Shoichi; Nakajima, Shuhei
Bioscience, Biotechnology, and Biochemistry, 1995 , vol. 59, # 2 p. 353 - 354
反应条件
(i) POCl3, Py, (ii) /BRN= 3563126/, Py; Multistep reaction;
参考文献
Shveits,V.I. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, p. 3983 - 3986,4042 - 4045
参考文献
Shvets,V.I. et al.
Chemistry of Natural Compounds, 1966 , vol. 2, p. 181 - 184
Khimiya Prirodnykh Soedinenii, 1966 , vol. 2, p. 225 - 229