1: thionyl chloride / benzene / 0.5 h / 60 °C 2: 101 mg / liquid ammonia / tetrahydrofuran / -78 - 17 °C View Scheme
参考文献
Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
1: thionyl chloride / benzene / 0.5 h / 60 °C
2: 101 mg / liquid ammonia / tetrahydrofuran / -78 - 17 °C
3: 81 percent / Lawesson's reagent / toluene / 1.5 h / Heating
4: 20 mg / sodium hydride, methyl iodide, water / tetrahydrofuran / 1 h / 50 °C
View Scheme
参考文献
Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
1: thionyl chloride / benzene / 0.5 h / 60 °C
2: 101 mg / liquid ammonia / tetrahydrofuran / -78 - 17 °C
3: 81 percent / Lawesson's reagent / toluene / 1.5 h / Heating
4: sodium hydride, methyl iodide, water / tetrahydrofuran / 1 h / 50 °C
View Scheme
参考文献
Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
1: thionyl chloride / benzene / 0.5 h / 60 °C
2: 42 percent / liquid ammonia / tetrahydrofuran / -78 - 17 °C
View Scheme
参考文献
Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
