3,3’-二硫代二丙酰甲胺合成路线 (共 13 条)
反应条件
sodium sulfite in water T=10°C; 24 h; Inert atmosphere; Product distribution / selectivity;
参考文献
SK Chemicals Co., Ltd.
Patent: US2012/330061 A1, 2012 ;
Location in patent: Page/Page column 7 ;
反应条件
1: SOCl2 / benzene / 4 h / Heating 2: CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 153 - 158
反应条件
in chloroform 24 h; Ambient temperature;
参考文献
Easton, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 153 - 158
参考文献
Justus Liebigs Annalen der Chemie, , vol. 679, p. 123 - 135
参考文献
Justus Liebigs Annalen der Chemie, , p. 1249 - 1266
反应条件
thionyl chloride in 1,2-dichloro-ethane
参考文献
Clerici, Francesca; Contini, Alessandro; Gelmi, Maria Luisa; Pocar, Donato
Tetrahedron, 2003 , vol. 59, # 47 p. 9399 - 9408
反应条件
pyridine; bromine in dichloromethane from -78 deg C to room temp.;
参考文献
Easton, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 153 - 158
反应条件
thionyl chloride in 1,2-dichloro-ethane T=10°C; 2 h;
参考文献
Clerici, Francesca; Contini, Alessandro; Gelmi, Maria Luisa; Pocar, Donato
Tetrahedron, 2003 , vol. 59, # 47 p. 9399 - 9408
反应条件
thionyl chloride in 1,2-dichloro-ethane
参考文献
Clerici, Francesca; Contini, Alessandro; Gelmi, Maria Luisa; Pocar, Donato
Tetrahedron, 2003 , vol. 59, # 47 p. 9399 - 9408
反应条件
sulfuryl dichloride in 1,2-dichloro-ethane
参考文献
Lewis,S.N. et al.
Journal of Heterocyclic Chemistry, 1971 , vol. 8, p. 571 - 580