in neat (no solvent) byproducts: NH3; heating (70-85°C, then 110-120°C, several h); distn. (vac.);
参考文献
Voronkov, M. G.; Mirskov, R. G.; Chernova, V. G.; Ivanova, N. P.
Journal of General Chemistry USSR (English Translation), 1981 , vol. 51, p. 1430 - 1430
Zhurnal Obshchei Khimii, 1981 , vol. 51, p. 1678 - 1678
n-butyllithium in diethyl ether; hexane T=20°C; 2 h;
参考文献
Lappert, Michael F.; Slade, Martin J.; Singh, Anirudh; Atwood, Jerry L.; Rogers, Robin D.; Shakir, Riz
Journal of the American Chemical Society, 1983 , vol. 105, # 2 p. 302 - 304