反应条件
in hexane (inert atmosphere, Schlenk technique); Sn-compd. is dissolved in hexane, solid H2NBMes2 is added slowly at room temp., soln. is refluxed for 1 h and then cooled; volatiles are removed under reduced pressure, residue is redissolved in hexane, filtn., reduction of volume, crystn.;
参考文献
Inorganic Chemistry, , vol. 30, p. 3390 - 3394
