反应条件
in toluene
byproducts: Me3SiCl, HCl; addn. of HN(SiMe3)2 to soln. of PhBCl2 (inert atmosphere), kept at 0°C for 30 min; warmed to ca 35°C, heated for 2 h at 120°C; cooling to room temp., volatiles removed (vac.), residue stirred overnight with hexane; insolubles collected, washed (hexane), dried (vac.): (BPhNH)3; filtrate concd., standing at room temp., ppt. collected, dried (vac.); elem. anal.;
参考文献
Niedenzu, Kurt; Serwatowska, Joanne; Serwatowski, Janusz
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1992 , vol. 47, # 5 p. 713 - 717
