N,N-二甲基对硝基苯胺合成路线 (共 150 条)
反应条件
1H-imidazole; 5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride in chloroform T=25°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 27, # 14 p. 1617 - 1620
反应条件
sodium hydroxide; tetrabutyl-ammonium chloride in toluene
参考文献
Synthetic Communications, , vol. 26, # 21 p. 4065 - 4080
反应条件
water; potassium carbonate; N,N-dimethyl-formamide T=135 - 140°C; 2.3 h; Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 5 p. 655 - 657
反应条件
water; potassium carbonate; N,N-dimethyl-formamide T=135 - 140°C; 2 h; Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 5 p. 655 - 657
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=160°C; 8 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 23, p. 1507 - 1509
反应条件
water; potassium carbonate; N,N-dimethyl-formamide T=135 - 140°C; 4.1 h; Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 5 p. 655 - 657
反应条件
1: 3-(5-amino-4-cyano-1H-imidazol-1-yl) benzoic acid With sodium nitrite in water; acetic acid T=0 - 5°C; 0.583333 h; 2: N,N-dimethyl-aniline in water; acetic acid T=20°C; 0.5 h; Further stages.;
参考文献
Journal of Heterocyclic Chemistry, , vol. 44, # 1 p. 13 - 19
反应条件
pyridine; sodium hydrogencarbonate
参考文献
Journal of the American Chemical Society, , vol. 71, p. 740
反应条件
water; potassium carbonate; N,N-dimethyl-formamide T=135 - 140°C; 8.1 h; Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 5 p. 655 - 657
反应条件
1: tetrakis(dimethylamino)diboron; 3-hydroxy-2,2-dimethylpropanol With potassium acetate in toluene T=80°C; 2: 4-nitrophenyl trifluoromethanesulphonate With tetrakis(triphenylphosphine) palladium(0) in toluene T=80°C; 22 h;
参考文献
Tetrahedron Letters, , vol. 53, # 46 p. 6230 - 6235,6