in melt stirring of 7.37 mmol triphenyltin hydride and 11 mmol 4-vinylpyridine at 100°C for 0.5 h as a melt under N2;; recrystallization from petroleum ether yields hexaphenylditin; evaporation of the mother liquor to dryness under reduced pressure; recrystallization from petroleum ether; elem. anal.;;
triphenylphosphine; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate in tetrahydrofuran Alkylation; 20 h; Heating;
参考文献
Beller, Matthias; Trauthwein, Harald; Eichberger, Martin; Breindl, Claudia; Mueller, Thomas E.
European Journal of Inorganic Chemistry, 1999 , # 7 p. 1121 - 1132
zirconocene dichloride in benzene T=150°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Selimov, F. A.; Ptashko, O. A.; Fatykhov, A. A.; Khalikova, N. R.; Dzhemilev, U. M.
Russian Chemical Bulletin, 1993 , vol. 42, # 5 p. 872 - 878
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 5 p. 916 - 921
ammonia; oxygen; vanadium pentoxide T=345°C; var. reaction rates; MechanismThermodynamic data;
参考文献
Vorob'ev, P. B.; Suvorov, B. V.; Shlygina, I. A.; Gabdrakipov, V. Z.; Mikhailovskaya, T. P.
Russian Journal of General Chemistry, 1993 , vol. 63, # 6.2 p. 931 - 934
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 6 p. 1332 - 1337
