1: benzyl alcohol With sodium hydride in tetrahydrofuran 2: (2-oxo-1,3-dioxolan-4-yl)methyl 4-methylbenzenesulfonate With tetrabutylammomium bromide in tetrahydrofuran T=-70 - 20°C;
1,4-diaza-bicyclo[2.2.2]octane in acetone Ambient temperature;
参考文献
Bakhtiar, Cuross; Smith, Edward H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 3 p. 239 - 244
1: benzyl alcohol With sodium hydride in tetrahydrofuran T=0°C; 1 h; 2: carbon dioxide in tetrahydrofuran T=0°C; 0.5 h; 3: benzyl chloroformate in tetrahydrofuran T=20°C; 18 h; Title compound not separated from byproducts;
参考文献
Davies, Stephen G.; Haggitt, Jane R.; Ichihara, Osamu; Kelly, Richard J.; Leech, Michael A.; Mortimer, Anne J. Price; Roberts, Paul M.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 18 p. 2630 - 2649
