反应条件
Et3N; (PPN)Cl in tetrahydrofuran Under N2, evapn. of volatiles from a Co-complex soln. (-20°C), addn. of fresh THF and PhMgBr, stirring (-20°C, 5 h; room temp., 2 h), addn. of Et3N, stirring overnight at room temp., metathesis with (PPN)Cl.; Monitored by (11)B-NMR, Et2O-sol. fraction yields B containing compounds.;
参考文献
Basil, John D.; Aradi, Allen A.; Bhattacharyya, Nripendra K.; Rath, Nigram P.; Eigenbrot, Charles; Fehlner, Thomas P.
Inorganic Chemistry, 1990 , vol. 29, p. 1260 - 1270