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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
溴化苯基镁
合成路线
（共 1496 条）
936-51-6
2-苯基-1,3-二四氢呋喃
+
100-58-3
溴化苯基镁
→
反应条件
91-01-0
二苯甲醇
反应条件
1: PhCH(OCH2CH2O) With triethylsilyl trifluoromethanesulphonate; triphenylphosphine in dichloromethane T=0°C; 0.5 h; Schlenk technique; 2: phenyl-magnesium bromide in dichloromethane T=0°C; Schlenk technique;
参考文献
Chemistry - A European Journal, , vol. 18, # 36 p. 11423 - 11432
936-51-6
2-苯基-1,3-二四氢呋喃
+
79271-56-0
三乙基硅基三氟甲磺酸酯
+
100-58-3
溴化苯基镁
+
603-35-0
三苯基磷
→
反应条件
91-01-0
二苯甲醇
反应条件
1: PhCH(OCH2CH2O); triethylsilyl trifluoromethanesulphonate; triphenylphosphine in dichloromethane T=0°C; 0.5 h; 2: phenyl-magnesium bromide With oxygen in dichloromethane T=0°C;
参考文献
Chemical Communications, , vol. 47, # 35 p. 9894 - 9896
100-52-7
苯甲醛
+
100-58-3
溴化苯基镁
→
反应条件
91-01-0
二苯甲醇
反应条件
Inert atmosphere;
参考文献
European Journal of Medicinal Chemistry, , vol. 44, # 3 p. 1223 - 1229
100-58-3
溴化苯基镁
→
反应条件
91-01-0
二苯甲醇
+
1454679-91-4
反应条件
1.1: diethyl ether / -78 - 20 °C 2.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 8 h / 0 - 60 °C 3.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 3.2: 20 °C 4.1: diethyl ether / -78 - 20 °C 5.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 24 h / 0 - 60 °C 6.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 6.2: 1 h / 0 - 20 °C View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1217 - 1225
100-58-3
溴化苯基镁
→
反应条件
91-01-0
二苯甲醇
+
5194-35-4
反应条件
1.1: diethyl ether / -78 - 20 °C 2.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 8 h / 0 - 60 °C 3.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 3.2: 20 °C 4.1: diethyl ether; hexane / -78 - 20 °C 5.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 8 h / 0 - 60 °C 6.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 6.2: 1 h / 0 - 20 °C View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1217 - 1225
100-58-3
溴化苯基镁
→
反应条件
91-01-0
二苯甲醇
反应条件
1.1: diethyl ether / -78 - 20 °C 2.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 24 h / 0 - 60 °C 3.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 3.2: 1 h / 0 - 20 °C View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1217 - 1225
68-12-2
+
100-58-3
溴化苯基镁
→
反应条件
108-86-1
+
100-52-7
苯甲醛
反应条件
1: phenyl-magnesium bromide in tetrahydrofuran; [TDTHP][Deca] T=-78 - 20°C; 2: N,N-dimethyl-formamide in [TDTHP][Deca]; hexane Product distribution / selectivity;
参考文献
SIMON FRASER UNIVERSITY
Patent: WO2006/7703 A1, 2006 ;
Location in patent: Page/Page column 23 ;
100-58-3
溴化苯基镁
→
反应条件
98-85-1
反应条件
1.1: diethyl ether / -78 - 20 °C 2.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 5 h / 0 - 60 °C 3.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 3.2: 1 h / 0 - 20 °C View Scheme
参考文献
Too, Pei Chui; Tnay, Ya Lin; Chiba, Shunsuke
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1217 - 1225
60-29-7
+
100-58-3
溴化苯基镁
→
反应条件
92-52-4
+
3299-05-6
+
100-41-4
+
98-85-1
+
108-88-3
+
71-43-2
反应条件
iodine 1.5 h; HeatingH2O quench, deuterium incorporation in D2O quench, other solvent systems; Product distributionMechanism;
参考文献
Jones, Louis A.; Kirby, Suzanne L.; Kean, David M.; Campbell, Gary L.
Journal of Organometallic Chemistry, 1985 , vol. 284, p. 159 - 170
7782-49-2
+
100-58-3
溴化苯基镁
→
反应条件
1666-13-3
反应条件
in diethyl ether RefluxInert atmosphere;
参考文献
Wang, Bingshuai; Yu, Fabiao; Li, Peng; Sun, Xiaofei; Han, Keli
Dyes and Pigments, 2013 , vol. 96, # 2 p. 383 - 390
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