acetic anhydride; iron in tetrahydrofuran stirring phenylhydroxylamine and Ph3BiCO3 for 30 min under Ar at room temp., reductive acetylation: iron powder, AcOH, (CH3CO)2O, 100°C, 2.5 h; work-up, t.l.c.;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 241 - 250
Barton, Derek H. R.; Finet, Jean-Pierre; Giannotti, Charles; Halley, Frank
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 241 - 250
BiPh3CO3 effect of spin trap; var. reaction cond.; Product distributionMechanism;
参考文献
Barton, Derek H. R.; Finet, Jean-Pierre; Giannotti, Charles; Halley, Frank
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 241 - 250
1: diethyl ether 2: sulfur trioxide / pyridine; CH2Cl2 / 120 h / Ambient temperature 3: 2.5 percent Chromat. / 0.5 M KCl / acetonitrile; H2O / 40 °C View Scheme
参考文献
Novak, Michael; Pelecanou, Maria; Roy, Ajit K.; Andronico, Anthony F.; Plourde, Francine M.; et al.
Journal of the American Chemical Society, 1984 , vol. 106, # 19 p. 5623 - 5631
benzeneseleninic anhydride in tetrahydrofuran 0.05 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Lester, David J.; Ley, Steven V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1212 - 1217
