1: methoxybenzene With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane T=-55 - 20°C; Metallation; 3 h; 2: N,N-dimethylcarbamoyl chloride in diethyl ether; hexane T=-50 - 0°C; Acylation; 3 h;
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Verkerk, Udo; Fujita, Megumi; Dzwiniel, Trevor L.; McDonald, Robert; Stryker, Jeffrey M.
Journal of the American Chemical Society, 2002 , vol. 124, # 34 p. 9988 - 9989
Gilman; Webb
Journal of the American Chemical Society, 1940 , vol. 62, p. 987
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Gilman; Bebb
Journal of the American Chemical Society, 1939 , vol. 61, p. 109 Anm.4
Journal of the American Chemical Society, 1940 , vol. 62, p. 987
1: diformylimide sodium salt With methanesulfonyl chloride in 1,2-dichloro-ethane T=20 - 25°C; 2 h; 2: methoxybenzene With AlCl3, aluminium chloride in 1,2-dichloro-ethane Fries rearrangement; 2 h; Reflux;
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Hashmi, Imran Ali; Kantlehner, Willi; Ivanov, Ivo C.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2008 , vol. 63, # 4 p. 478 - 480
