反应条件
in neat (no solvent)
addn. of diborane to amine at liquid N2 temp., keeping at -111°C, -78°C and 0°C consecutively, stirring at 0°C for 4-6 h (vacuum line); cooling to -78°C, removal of B2H6 by distn.;
参考文献
Brown, Herbert C.; Murray, Leo T.
Inorganic Chemistry, 1984 , vol. 23, p. 2746 - 2753
