in neat (no solvent) passing a stream of Cl2 and S2Cl2 over hot starting material;;
参考文献
Bourion
Ann. Chim. Phys., 1910 , vol. 20, p. 547 - 547
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Matignon; Bourion
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1904 , vol. 138, p. 631 - 631
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Matignon
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 140, p. 1181 - 1181
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Gmelin Handbook: Cl: MVol., 65, page 183 - 186
silica gel in neat (no solvent) byproducts: SiCl4; react. of Ca3(PO4)2 with S2Cl2 at 1000 °C in presence of SiO2;; after 1 h 9.5 percent phosphate are caused to react.;;
Woehler,; Hiller,
Ann. Chim. Phys., 1855 , vol. 44, p. 56 - 57
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Woehler,; Hiller,
Justus Liebigs Annalen der Chemie, 1855 , vol. 93, p. 274 - 276
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Gmelin Handbook: P: MVol.B, 3.4.2.2, page 307 - 310