in neat (no solvent) heated in Pt crucible in a helium flow (150 ml/min) at a rate of 10 K/min to 450°C; washed (H2O); dried; monitored by IR spectroscopy;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 49, # 8 p. 1148 - 1153
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 104, p. 223 - 223
Cl: MVol., 65, page 183 - 186
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反应条件
in neat (no solvent) Kinetics; chlorination of chromite mineral at 900-1040°C for 2 h; detd. by X-ray diffraction, scanning electron microscopy and chem. anal.; monitored by TGA;
