in solid matrix Irradiation (UV/VIS); photolysis of solid matrix Ar:OCS:PCl3=100:1:1 using unfiltered emission of Hg arc 20 K for 60 min;; not isolated; detn. in solid matrix by IR spectroscopy;;
参考文献
Journal of Physical Chemistry, , vol. 89, # 15 p. 3326 - 3334
in further solvent(s) (argon); refluxing PCl5 and (NH4)2SO4 1 h in tetrachloroethane, removal of volatiles (vac.), after cooling addn. of SO2; filtration, removal of solvent (vac.), purifn. by microdistn.;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 51, # 8 p. 1079 - 1083
