exothermic react.; removing C4H9Cl and OPCl3 at reduced pressure, distn. of residue;
参考文献
Mikhailov, B. M.; Shchegoleva, T. A.
Bull. Acad. Sci. USSR Div. Chem. Sci., 1956 , p. 501 - 502
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Gmelin Handbook: B: B-Verb.9, 6.2.3, page 280 - 286
in hexane Ar atmosphere, addn. of B-compound to soln. of PCl5 (during 40 min, 50°), stirring (2 h); solvent and POCl3 removal (14 Torr, <40°C), distn.;
