反应条件
in dichloromethane addn. of CH2Cl2 to SbCl3 and (Et4N)2Fe4(CO)13 in a Schlenk flask and stirring overnight, filtration, all operations under N2; removal of solvent in vacuo, extraction with Et2O until soln. nearly colorless, removal of solvent, washing with hexane, drying in vacuo;
参考文献
Whitmire, Kenton H.; Leigh, J. Scott; Luo, Shifang; Shieh, Minghuey; Fabiano, Michael D.; Rheingold, Arnold L.
New Journal of Chemistry, 1988 , vol. 12, p. 397 - 404