反应条件
aq. NH4Cl in tetrahydrofuran
dropwise addn. of soln. of SbCl3 in THF to cold soln. of stoich. amt. of BrMgCCPh in THF (-15°C, under N2), allowed to warm up, stirred (20°C, 2 h), hydrolysis with 10percent aq. NH4Cl (-10°C), extn. with ether; ext. washed with satd. NaCl-soln., dried with Na2SO4, evapn. of solvent in high vac.;
参考文献
Lang, Heinrich; Zsolnai, Laszlo
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1990 , vol. 45, # 11 p. 1529 - 1536
