in further solvent(s) NH4Cl reacted with PCl5 in 1,1,2,2-tetrachloroethane according to L. G. Lund, N. L. Paddock, J. E. Proctor, H. T. Searle, Journal of the Chemical Society (1960) 2542; vac. distilled on Vigreux column;
参考文献
Vorontsov, Ivan I.; Tur, Dzidra R.; Papkov, Vladimir S.; Antipin, Mikhail Yu.
Journal of Molecular Structure, 2009 , vol. 928, # 1-3 p. 1 - 11
in trichlorophosphate byproducts: Cl2(O)P(NPCl2)5Cl; under reflux; treatment of the crude product with n-heptane, products identified in the sol. and in the insol. phase with NMR spectroscopy;
参考文献
Abouchaccra, Taher; Helioui, Moncef; Puskaric, Emile; Jaeger, Roger de; Heubel, Joseph
Journal of Chemical Research, Synopses, 1981 , p. 230 - 231
