Schmeisser, M.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1947 , vol. 255, p. 33 - 44
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Gmelin Handbook: Cl: SVol.B2, 96, page 523 - 524
water in water hydrolysis on heating with an excess of H2O; formation of POCl3, P2O3Cl4 and P2O5; amount of P2O5 increased with increasing ratio H2O:PCl5;;
in further solvent(s) byproducts: SO2, Cl2, HCl; refluxing PCl5 and (NH4)2SO4 in 1,1,2,2-tetrachloroethane for 12 h; cooling, washing with CCl4 or petroleum ether, elem. anal.;
参考文献
Helioui, Moncef; Chakra, Taher Abou; Jaeger, Roger de; Heubel, Joseph
Revue de Chimie Minerale, 1983 , vol. 20, p. 45 - 53
in neat (no solvent) react. with P2O3Cl4 at water bath temp.;;
参考文献
Geuther, A.; Michaelis, A.
Jena. Z. Med. Naturwiss., 1873 , vol. 7, p. 103 - 109
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Geuther, A.; Michaelis, A.
Ber., 1871 , vol. 4, p. 766 - 768
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Gmelin Handbook: P: MVol.C, 200, page 458 - 460
