in neat (no solvent) passing POCl3/HBr through a tube, packed with pumice, at 400 to 500°C;; fractionating;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1896 , vol. 122, p. 814 - 817
Full Text Show Details
Gmelin Handbook: P: MVol.C, 225, page 516 - 517
in not given formation only in big excess of HBr and pyridine, pptn. after concn. of mixt. on a waterbath and cooling;; filtration, washing with alcohol;;
参考文献
Meyer, J.; Hoehne, K.
Z. Anorg. Chem., 1937 , vol. 231, p. 372 - 372
Full Text Show Details
Gmelin Handbook: Rh: MVol., 38, page 92 - 94
→
反应条件
in water boiling concd. HBr soln.;;
参考文献
Poulenc. P.
Annales de Chimie (Cachan, France), 1935 , vol. 4, p. 617 - 617
Full Text Show Details
Gmelin Handbook: Rh: MVol., 65, page 147 - 149
Chattaway, F. D.; Wadmore, J. M.
Journal of the Chemical Society, 1902 , vol. 81, p. 197 - 197
Full Text Show Details
Gmelin Handbook: I: MVol.2, 96, page 456 - 457
Solomatin, V. S.; Kuz'min, N. M.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1981 , vol. 26, p. 390 - 394
Zhurnal Neorganicheskoi Khimii, 1981 , vol. 26, p. 726 - 733
