triethylamine in diethyl ether; ethanol a soln. of GeCl4 in dry Et2O was added dropwise to a stirred mixt. of abs. EtOH and Et3N in Et2O, stirred for 24 h; filtered, the soln. was distd.;
参考文献
Mazerolles, Pierre; Gregoire, Fabienne
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1986 , vol. 16, p. 905 - 914
in ethanol reaction of a alcoholic soln. of Na with GeCl4;;
参考文献
Taubern, D. L.; Orndorff, W. R.; Dennis, L. M.
Journal of the American Chemical Society, 1925 , vol. 47, p. 2039 - 2044
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Gmelin Handbook: Ge: MVol., 20, page 53 - 57
