2-甲氧基-5,5-二甲基-1,3,2-二氧磷杂环己烷合成路线 （共 26 条）
反应条件
1: 65.8 percent / diethyl ether / 7 h / Heating 2: 31 percent / piperidine, acetic acid / benzene / 6.5 h / Heating View Scheme
参考文献
Sakoda; Kamikawaji; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2362 - 2369
反应条件
in chlorobenzene T=29.9°C; Rate constantMechanism;
参考文献
Koenig, T.; Habicher, W. D.; Schwetlick, K.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 6 p. 913 - 922
参考文献
Tetrahedron, , vol. 20, p. 2781 - 2795
参考文献
Bartle,K.D. et al.
Tetrahedron, 1967 , vol. 23, p. 1701 - 1711
反应条件
1: 65.8 percent / diethyl ether / 7 h / Heating 2: 31 percent / piperidine, acetic acid / benzene / 6.5 h / Heating 3: 45 percent / toluene / 5 h / Heating View Scheme
参考文献
Sakoda; Kamikawaji; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2362 - 2369
反应条件
triethylamine; phosphorus trichoride
T=100°C;
参考文献
Morita; Kunimoto; Tsuda; Tada; Kise; Kimura
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 10 p. 4144 - 4154
反应条件
pyridine in diethyl ether
参考文献
Edmundson,R.S.
Tetrahedron, 1964 , vol. 20, p. 2781 - 2795
反应条件
1: 75 percent / Na / dioxane / 24 h / 20 °C
2: -50 °C
View Scheme
参考文献
Nifant'ev, E. E.; Grachev, M. K.; Bekker, A. R.; Vasyanina, L. K.; Koroteev, A. M.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 2 p. 312 - 316,274 - 278
参考文献
Sakoda; Kamikawaji; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2362 - 2369
反应条件
triethylamine in benzene
参考文献
Motoyoshiya, Jiro; Ikeda, Tsuneaki; Tsuboi, Shuji; Kusaura, Tatsuya; Takeuchi, Yoshino; Hayashi, Satoko; Yoshioka, Sachiko; Takaguchi, Yutaka; Aoyama, Hiromu
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 5950 - 5955
