2,2,6,6-四氘代环已酮合成路线 (共 3 条)
反应条件
water-d2; potassium carbonate 62 h; Heating;
参考文献
Pellicciari, Roberto; Natalini, Benedetto; Sadeghpour, Bahman M.; Marinozzi, Maura; Snyder, James P.; Williamson, Bobby L.; Kuethe, Jeffrey T.; Padwa, Albert
Journal of the American Chemical Society, 1996 , vol. 118, # 1 p. 1 - 12
反应条件
water-d2; trichlorophosphate 20 grad C, 3 d; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Grishina, G. V.; Leshcheva, I. F.; Sergeev, N. M.; Potapov, V. M.; Vovk, A. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 6 p. 589 - 593
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 6 p. 780 - 784
反应条件
in gas byproducts: Fe(CD2CO)(1+), Fe(C5D4H4)(1+), Fe(C5D4H6)(1+); other byproducts are:C5D4H6, C4D2H6, H2, CD2CO and CO, from 1E-7 to 2E-6 Torr; in ion cyclotron resonance spectrometer;
参考文献
Burnier, R.C.; Byrd, G.D.; Freiser, B.S.
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4360 - 4367