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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5-甲氧基吲哚
合成路线
（共 219 条）
1006-94-6
5-甲氧基吲哚
+
106-96-7
3-溴丙炔
→
反应条件
475473-79-1
5-甲氧基-1-(2-丙炔-1-基)-1H-吲哚
反应条件
tetra-(n-butyl)ammonium iodide; sodium hydride in N,N-dimethyl-formamide T=0 - 70°C; 8.25 h; Heating / reflux;
参考文献
INDUSTRY-ACADEMIC COOPERATION FOUNDATION, YONSEI UNIVERSITY
Patent: WO2008/117935 A1, 2008 ;
Location in patent: Page/Page column 36 ;
1006-94-6
5-甲氧基吲哚
→
反应条件
56366-26-8
反应条件
2,6-di-tert-butyl-pyridine; copper(II) bis(trifluoromethanesulfonate) in dichloromethane T=20°C; 14 h;
参考文献
Phipps, Robert J.; Grimster, Neil P.; Gaunt, Matthew J.
Journal of the American Chemical Society, 2008 , vol. 130, # 26 p. 8172 - 8174
1006-94-6
5-甲氧基吲哚
+
108-94-1
环己酮
→
反应条件
56366-26-8
反应条件
palladium (II) trifluoroacetate; oxygen; bis[2-(diphenylphosphino)phenyl] ether in toluene T=140°C; 30 h; regioselective reaction;
参考文献
Chen, Shanping; Liao, Yunfeng; Zhao, Feng; Qi, Hongrui; Liu, Saiwen; Deng, Guo-Jun
Organic Letters, 2014 , vol. 16, # 6 p. 1618 - 1621
1006-94-6
5-甲氧基吲哚
+
108-86-1
溴代苯
→
反应条件
56366-26-8
反应条件
potassium carbonate; [(t-Bu)2P(OH)]2PdCl2 in 1,4-dioxane 24 h; Heating;
参考文献
Zhang, Zhiqiang; Hu, Zhizhi; Yu, Zhixiao; Lei, Peng; Chi, Haijun; Wang, Yue; He, Ren
Tetrahedron Letters, 2007 , vol. 48, # 13 p. 2415 - 2419
1006-94-6
5-甲氧基吲哚
+
108-86-1
溴代苯
→
反应条件
56366-26-8
+
5883-96-5
5-甲氧基-2-苯基-1H-吲哚
反应条件
lithium hydroxide hydrate; palladium diacetate; bis(1,1-diphenylphosphino)methane in water T=110°C; 18 h; regioselective reaction;
参考文献
Joucla, Lionel; Batail, Nelly; Djakovitch, Laurent
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2929 - 2936
1006-94-6
5-甲氧基吲哚
+
100-63-0
苯肼
→
反应条件
56366-26-8
反应条件
1,10-phenanthroline; palladium diacetate; trifluoroacetic acid in chlorobenzene T=100°C; 12 h;
参考文献
Chen, Yongxin; Guo, Shuaibo; Li, Kangning; Qu, Jinpeng; Yuan, Hua; Hua, Qiuru; Chen, Baohua
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 711 - 715
1006-94-6
5-甲氧基吲哚
+
98-09-9
苯磺酰氯
→
反应条件
56995-12-1
反应条件
1: 5-Methoxy-1H-indole With sodium hydride in tetrahydrofuran; mineral oil T=0°C; 0.333333 h; Inert atmosphere; 2: benzenesulfonyl chloride in tetrahydrofuran; mineral oil T=0 - 20°C; Inert atmosphere;
参考文献
Chen, Jianjun; Li, Chien-Ming; Wang, Jin; Ahn, Sunjoo; Wang, Zhao; Lu, Yan; Dalton, James T.; Miller, Duane D.; Li, Wei
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 16 p. 4782 - 4795
1006-94-6
5-甲氧基吲哚
→
反应条件
56995-12-1
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogen sulphate; benzenesulfonyl chloride in dichloromethane
参考文献
Sanofi
Patent: US5079363 A1, 1992 ;
1006-94-6
5-甲氧基吲哚
→
反应条件
56995-12-1
反应条件
n-butyllithium; benzenesulfonyl chloride in tetrahydrofuran; [2,2']bipyridinyl; hexane
参考文献
Merck and Co., Inc.
Patent: US4840963 A1, 1989 ;
1006-94-6
5-甲氧基吲哚
+
105-36-2
溴乙酸乙酯
→
反应条件
57000-49-4
反应条件
1: 5-Methoxy-1H-indole With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.25 h; 2: With zinc(II) chloride in tetrahydrofuran; diethyl ether; hexane 24 h; 3: ethyl bromoacetate in toluene 24 h;
参考文献
Boularot, Adrien; Giglione, Carmela; Petit, Sylvain; Duroc, Yann; De Sousa, Rodolphe Alves; Larue, Valery; Cresteil, Thierry; Dardel, Frederic; Artaud, Isabelle; Meinnel, Thierry
Journal of Medicinal Chemistry, 2007 , vol. 50, # 1 p. 10 - 20
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