(2,2-二甲基丙基)苯合成路线 (共 75 条)
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in diethyl ether Heating;
参考文献
Tetrahedron Letters, , vol. 32, # 2 p. 189 - 192
反应条件
sodium tetrahydroborate in methanol; ethanol 2 h;
参考文献
Journal of Organic Chemistry, , vol. 51, # 8 p. 1341 - 1346
反应条件
1: 1-iodo-2,2-dimethylpropane With [Fe(C2H4)4][Li(tmeda)]2 in tetrahydrofuran 2: phenyl magnesium halide in tetrahydrofuran; diethyl ether T=0°C; 4 h; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 130, # 27 p. 8773 - 8787
反应条件
1,3-bis-(diphenylphosphino)propane; CoCl2 in tetrahydrofuran T=0°C; 2 h;
参考文献
Chemistry - A European Journal, , vol. 10, # 22 p. 5640 - 5648
反应条件
1: phenyl-magnesium bromide With zinc(II) chloride in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 2: With methyl-magnesium chloride in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: 1-iodo-2,2-dimethylpropane With triphenylphosphine; nickel dichloride in tetrahydrofuran T=0 - 20°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 52, # 52 p. 7087 - 7090
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran T=-78 - 67°C;
参考文献
Journal of Organic Chemistry, , vol. 55, # 25 p. 6188 - 6194
反应条件
silver trifluoromethanesulfonate in acetonitrile T=25°C; 0.5 h; Inert atmosphere;
参考文献
Chemistry - An Asian Journal, , vol. 5, # 6 p. 1487 - 1493
反应条件
ortho-chlorotoluene; sodium T=350°C; P=147102 Torr;
参考文献
Journal of the American Chemical Society, , vol. 78, p. 4316,4317, 4322
反应条件
18-crown-6 ether in dimethyl sulfoxide T=35°C; Irradiation;
参考文献
Journal of the American Chemical Society, , vol. 107, # 5 p. 1450 - 1452
反应条件
1: phenyl-magnesium bromide With ZnI2(tmeda) in tetrahydrofuran 2: 2,2-dimethyl-1-propyl p-toluenesulfonate With anhydrous iron chloride in tetrahydrofuran T=0 - 50°C;
参考文献
Organic Letters, , vol. 11, # 19 p. 4306 - 4309