1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate; magnesium sulfate in N,N-dimethyl-formamide T=105°C;

1: 1-bromocyclohexane With chloro-trimethyl-silane; magnesium; ethylene dibromide; lithium chloride; zinc dibromide in tetrahydrofuran T=0 - 25°C; 4 h; Inert atmosphere; 2: With zinc dibromide in tetrahydrofuran T=25°C; 0.166667 h; Inert atmosphere; 3: cyano derivative of benzenediazonium tetrafluoroborate With chloro-trimethyl-silane in tetrahydrofuran T=-60 - 125°C; Inert atmosphereMicrowave irradiation; regioselective reaction;

in acetic acid 4 h; Reflux;

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hydrogenchloride

acetic acid Reflux;