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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-苯基吡啶
合成路线
（共 190 条）
108-86-1
溴代苯
+
59020-10-9
3-(三正丁基锡)吡啶
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
copper(l) iodide; C37H51ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide T=80°C; Stille Cross Coupling; 12 h; Inert atmosphere; SolventReagent/catalystTemperature;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
591-50-4
碘苯
+
59020-10-9
3-(三正丁基锡)吡啶
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
copper(l) iodide; C37H51ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide T=20°C; Stille Cross Coupling; 12 h; Inert atmosphere; Temperature;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
59020-10-9
3-(三正丁基锡)吡啶
+
108-90-7
氯苯
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
copper(l) iodide; C52H67ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide T=110°C; Stille Cross Coupling; 12 h; Inert atmosphere; TemperatureReagent/catalyst;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
1120-90-7
3-碘吡啶
+
71-43-2
苯
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
potassium tert-butylate in dimethyl sulfoxide T=20°C; 1 h; Schlenk techniqueInert atmosphereIrradiation;
参考文献
Bhakuni, Bhagat Singh; Yadav, Abhimanyu; Kumar, Shailesh; Kumar, Sangit
New Journal of Chemistry, 2014 , vol. 38, # 2 p. 827 - 836
108-86-1
溴代苯
+
59020-09-6
3-(三甲基锡烷基)-吡啶
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
copper(l) iodide; C37H51ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide T=80°C; Stille Cross Coupling; 12 h; Inert atmosphere;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
626-55-1
3-溴吡啶
+
960-16-7
三丁基苯基锡
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
cesium fluoride; palladium (II) trifluoroacetate in 1,4-dioxane T=100°C; Stille cross-coupling; 10 h;
参考文献
Gajare, Anil S.; Jensen, Rader S.; Toyota, Kozo; Yoshifuji, Masaaki; Ozawa, Fumiyuki
Synlett, 2005 , # 1 art. no. U25204ST, p. 144 - 148
626-55-1
3-溴吡啶
+
780-69-8
苯基三乙氧基硅烷
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
sodium hydroxide; palladium diacetate T=60°C; Hiyama reaction; 6 h;
参考文献
Shi, Shengyin; Zhang, Yuhong
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5927 - 5930
52843-75-1
+
98-80-6
苯硼酸
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
potassium phosphate; (NC5H3(N2C7H4(CH2)3CH3)2)NiBr(1+)*Br(1-)=Ni(NC5H3(N2C7H4(CH2)3CH3)2)Br2; triphenylphosphine in 1,4-dioxane T=100°C; Suzuki-Miyaura coupling; 24 h;
参考文献
Tu, Tao; Mao, Han; Herbert, Christian; Xu, Mizhi; Doetz, Karl Heinz
Chemical Communications, 2010 , vol. 46, # 41 p. 7796 - 7798
626-60-8
3-氯吡啶
+
2633-57-0
(三-2-丙烯-1-基硅烷基)-苯
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: 3-chloro-pyridine With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 14 h;
参考文献
Sahoo, Akhila K.; Nakao, Yoshiaki; Hiyama, Tamejiro
Chemistry Letters, 2004 , vol. 33, # 5 p. 632 - 633
51581-40-9
3-吡啶氨基甲酸二乙酯
+
98-80-6
苯硼酸
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
1: 3,4,5-trimethoxyphenylboronic acid T=75°C; 1 h; dehydrationvacuum; 2: 3-(N,N-diethylcarbamoyloxy)-pyridine With potassium phosphate; NiCl2(PCy3)2; PCy3∙HBF4 in o-xylene T=150°C; Suzuki-Miyaura coupling; 5 h; Inert atmosphere;
参考文献
Antoft-Finch, Aurora; Blackburn, Tom; Snieckus, Victor
Journal of the American Chemical Society, 2009 , vol. 131, # 49 p. 17750 - 17752
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