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乙二醇
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63148-62-9
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碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-苯基吡啶
合成路线
（共 190 条）
1132-27-0
+
98-80-6
苯硼酸
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki coupling; Inert atmosphere;
参考文献
Chen, Guo-Jun; Han, Fu-She
European Journal of Organic Chemistry, 2012 , # 19 p. 3575 - 3579
626-55-1
3-溴吡啶
+
201230-82-2
+
98-80-6
苯硼酸
→
反应条件
1008-88-4
3-苯基吡啶
+
5424-19-1
3-苯甲酰基吡啶
反应条件
[(P{(C6H11)3})2Pd(Cl)2] in tetrahydrofuran T=120°C; P=3750.3 Torr; 20 h;
参考文献
Tetrahedron Letters, , vol. 42, # 22 p. 3689 - 3691
4595-59-9
5-溴嘧啶
+
98-80-6
苯硼酸
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in PEG 300 T=55°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Silva, Aires da Conceicao; Senra, Jaqueline Dias; Aguiar, Lucia C.S.; Simas, Alessandro B.C.; Souza, Andrea Luzia F. de; Malta, Luiz Fernando Brum; Antunes
Tetrahedron Letters, 2010 , vol. 51, # 30 p. 3883 - 3885
1120-90-7
3-碘吡啶
+
780-69-8
苯基三乙氧基硅烷
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
palladium 10 on activated carbon; tetrabutyl ammonium fluoride; water; tris(p-fluoro phenyl)phosphine in toluene T=120°C; Hiyama coupling; 12 h; Inert atmosphere;
参考文献
Monguchi, Yasunari; Yanase, Takayoshi; Mori, Shigeki; Sajiki, Hironao
Synthesis (Germany), 2013 , vol. 45, # 1 art. no. SS-2012-Z0714-PSP, p. 40 - 44
1132-27-0
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
626-60-8
3-氯吡啶
+
108-86-1
溴代苯
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
bis(carbene)-derived nickel(II)-pincer complex in tetrahydrofuran T=20°C; Grignard coupling reaction; 48 h;
参考文献
Inamoto, Kiyofumi; Kuroda, Jun-Ichi; Sakamoto, Takao; Hiroya, Kou
Synthesis, 2007 , # 18 p. 2853 - 2861
626-60-8
3-氯吡啶
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [NiCl2(1,2-dimethoxyethane)]; caesium carbonate; zinc; tri-cyclo-hexyl-phosphine in N,N-dimethyl-formamide; acetone T=20 - 60°C; Suzuki-Miyaura cross-coupling reaction; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Chemical Communications, , vol. 47, # 1 p. 307 - 309
626-55-1
3-溴吡啶
+
960-16-7
→
反应条件
1008-88-4
3-苯基吡啶
+
92-52-4
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=110°C; Stille cross-coupling; 48 h; Inert atmosphere;
参考文献
Journal of Organometallic Chemistry, , vol. 695, # 1 p. 103 - 110
72253-33-9
+
98-80-6
苯硼酸
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
potassium phosphate; Ni(PCy3)2Cl2 in 1,4-dioxane T=110°C; Suzuki-Miyaura coupling; 24 h; Inert atmosphere;
参考文献
Chen, Hu; Huang, Zhongbin; Hu, Xiaoming; Tang, Guo; Xu, Pengxiang; Zhao, Yufen; Cheng, Chien-Hong
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 2338 - 2344
626-55-1
3-溴吡啶
+
1078-58-6
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
catalyst 1 (aliphatic, phosphine based pincer complex of palladium) in 1,4-dioxane; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 1.5 h;
参考文献
Gerber, Roman; Blacque, Olivier; Frech, Christian M.
Dalton Transactions, 2011 , vol. 40, # 48 p. 12939 - 12941
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