6-(4-甲基苯基)-6-氧代己酸合成路线 （共 15 条）
反应条件
1: 1.) O3, 2.) Me2S / 1.) CH2Cl2, 2.) -78 deg C 2: acetone / Jones oxidation View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1324 - 1325
反应条件
sodium hydroxide; thionyl chloride; aluminium trichloride in methanol; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; dichloromethane; water; toluene
反应条件
jones reagent in acetone T=0°C; 0.5 h; Yield given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 193 - 200
反应条件
chromium(VI) oxide; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 70, p. 1976
反应条件
1: p-TsOH / benzene / 16 h / Heating 2: 1.) O3, 2.) Me2S / 1.) CH2Cl2, -78 deg C, 10 min, 2.) -78 deg C to room t. 3: Jones reagent / acetone / 0.5 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 193 - 200
反应条件
1: 1.) Mg / 1.) THF, room t., 2.) THF, room t., 1 h 2: p-TsOH / benzene / 16 h / Heating 3: 1.) O3, 2.) Me2S / 1.) CH2Cl2, -78 deg C, 10 min, 2.) -78 deg C to room t. 4: Jones reagent / acetone / 0.5 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 193 - 200
反应条件
aluminium trichloride in toluene 12 h; Ambient temperature;
参考文献
Sudalai, A.; Rao, G.S.Krishna
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, p. 219 - 222
反应条件
aluminium trichloride; toluene Erwaermen des Reaktionsprodukts mit wss.-aethanol. KOH;
参考文献
Monatshefte fuer Chemie, , vol. 88, p. 517,527
反应条件
carbon disulfide; aluminium trichloride
参考文献
Chemische Berichte, , vol. 52, p. 2079
参考文献
Journal of the American Chemical Society, , vol. 70, p. 1976
