N-(叔丁基)-3-氯丙酰胺合成路线 (共 4 条)
反应条件
sodium hydroxide in dichloromethane; water T=-20 - 20°C; 2 h;
参考文献
MEDIVATION TECHNOLOGIES, INC.
Patent: WO2009/94668 A1, 2009 ;
Location in patent: Page/Page column 171 ;
WO 2009/094668 A1
反应条件
Polyvinylpolypyrrolidone-Supported Boron Trifluoride (PVPP-BF3) in 1,2-dichloro-ethane T=70°C; 3 h;
参考文献
Mokhtary, Masoud; Najafizadeh, Faranak
E-Journal of Chemistry, 2012 , vol. 9, # 2 p. 576 - 582
反应条件
HY zeolite exchanged using rare earth chloride mixture T=100°C; Addition; 24 h;
参考文献
Deshmukh, A. R. A. S.; Gumaste, V. K.; Bhawal, B. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1997 , vol. 36, # 4 p. 369 - 371
反应条件
thionyl chloride 1) dichloromethane, 3h, reflux, 2) dichloromethane, 3h, roomtemp.; Yield given. Multistep reaction;
参考文献
Easton, Christopher J.; Love, Stephen G.; Wang, Peng
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 2 p. 277 - 282